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Information card for entry 4066334
Preview
Coordinates | 4066334.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C29 H35 Fe N O2 P2 |
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Calculated formula | C29 H35 Fe N O2 P2 |
SMILES | [Fe]12345678([c]9(P(OCC)OCC)[c]1([c]2(P(c1ccccc1)c1ccccc1)[cH]3[cH]49)CN(C)C)[cH]1[cH]5[cH]6[cH]7[cH]81 |
Title of publication | Synthesis of Racemic Aminoalkylferrocenyldichlorophosphanes and -dialkylphosphonites and Their Conversion to Primary Phosphanes† |
Authors of publication | Limburg, Carolin; Lönnecke, Peter; Gómez-Ruiz, Santiago; Hey-Hawkins, Evamarie |
Journal of publication | Organometallics |
Year of publication | 2010 |
Journal volume | 29 |
Journal issue | 21 |
Pages of publication | 5427 |
a | 9.9909 ± 0.0002 Å |
b | 10.5284 ± 0.0002 Å |
c | 13.2106 ± 0.0002 Å |
α | 92.11 ± 0.001° |
β | 93.214 ± 0.001° |
γ | 103.366 ± 0.001° |
Cell volume | 1348.06 ± 0.04 Å3 |
Cell temperature | 130 ± 2 K |
Ambient diffraction temperature | 130 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0385 |
Residual factor for significantly intense reflections | 0.0314 |
Weighted residual factors for significantly intense reflections | 0.0906 |
Weighted residual factors for all reflections included in the refinement | 0.0927 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.089 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4066334.html
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