Information card for entry 4066356

Structure parameters

• Common name: in manuscript 5b
• Formula: C23 H41 Cl N3 P2 Rh
• Calculated formula: C23 H41 Cl N3 P2 Rh
• Title of publication: Neutralcis-Alkyl Olefin Rhodium(I) Complexes: Models of Intermediates in Late Transition Metal Olefin Polymerization with Surprising Structure†
• Authors of publication: Urtel, Heiko; Meier, Claudia; Rominger, Frank; Hofmann, Peter
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 21
• Pages of publication: 5496
• a: 10.8889 ± 0.0001 Å
• b: 15.4067 ± 0.0002 Å
• c: 16.1672 ± 0.0001 Å
• α: 90°
• β: 95.629 ± 0.001°
• γ: 90°
• Cell volume: 2699.16 ± 0.05 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0341
• Residual factor for significantly intense reflections: 0.0221
• Weighted residual factors for significantly intense reflections: 0.0481
• Weighted residual factors for all reflections included in the refinement: 0.0518
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No