Information card for entry 4066382

Structure parameters

• Formula: C42 H64 O13 Os P4 Sn
• Calculated formula: C42 H64 O13 Os P4 Sn
• SMILES: [OsH]([Sn](OC=O)(OC=O)O)([P](c1ccccc1)(OCC)OCC)([P](c1ccccc1)(OCC)OCC)([P](OCC)(OCC)c1ccccc1)[P](OCC)(OCC)c1ccccc1
• Title of publication: Reactivity of Dihydrides MH2P4(M = Fe, Ru, Os) with SnCl2: Preparation of Bis(trihydridestannyl) Derivatives
• Authors of publication: Albertin, Gabriele; Antoniutti, Stefano; Castro, Jesús
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 17
• Pages of publication: 3808
• a: 12.4488 ± 0.0008 Å
• b: 24.8116 ± 0.0015 Å
• c: 16.4851 ± 0.001 Å
• α: 90°
• β: 91.081 ± 0.001°
• γ: 90°
• Cell volume: 5090.9 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0718
• Residual factor for significantly intense reflections: 0.0387
• Weighted residual factors for significantly intense reflections: 0.0742
• Weighted residual factors for all reflections included in the refinement: 0.0868
• Goodness-of-fit parameter for all reflections included in the refinement: 0.993
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No