Information card for entry 4066397

Structure parameters

• Formula: C53 H68 N2 O3.5 Si
• Calculated formula: C53 H68 N2 O3.5 Si
• Title of publication: Base-Stabilized 1-Silacyclopenta-2,4-dienylidenes
• Authors of publication: Gao, Yihua; Zhang, Jianying; Hu, Hongfan; Cui, Chunming
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 14
• Pages of publication: 3063
• a: 13.436 ± 0.007 Å
• b: 13.62 ± 0.007 Å
• c: 15.581 ± 0.007 Å
• α: 92.464 ± 0.005°
• β: 111.247 ± 0.004°
• γ: 113.704 ± 0.006°
• Cell volume: 2373 ± 2 ų
• Cell temperature: 113 ± 2 K
• Ambient diffraction temperature: 113 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0947
• Residual factor for significantly intense reflections: 0.0778
• Weighted residual factors for significantly intense reflections: 0.1972
• Weighted residual factors for all reflections included in the refinement: 0.21
• Goodness-of-fit parameter for all reflections included in the refinement: 1.069
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No