Information card for entry 4066448

Structure parameters

• Formula: C27 H58 O Si5
• Calculated formula: C27 H58 O Si5
• Title of publication: Reactions of an Isolable Dialkylsilylene with Ketones†
• Authors of publication: Ishida, Shintaro; Iwamoto, Takeaki; Kira, Mitsuo
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 21
• Pages of publication: 5526
• a: 10.409 ± 0.002 Å
• b: 18.12 ± 0.004 Å
• c: 28.274 ± 0.006 Å
• α: 82.639 ± 0.002°
• β: 85.349 ± 0.003°
• γ: 84.839 ± 0.003°
• Cell volume: 5254.3 ± 1.9 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0762
• Residual factor for significantly intense reflections: 0.0625
• Weighted residual factors for significantly intense reflections: 0.1416
• Weighted residual factors for all reflections included in the refinement: 0.1479
• Goodness-of-fit parameter for all reflections included in the refinement: 1.179
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No