Information card for entry 4066606

Structure parameters

• Formula: C40 H48 Si
• Calculated formula: C40 H48 Si
• Title of publication: Reactions of (Et2NCH2CH2NEt2)·H2SiCl2with Selected Diorganometallic Reagents of Magnesium and Lithium†
• Authors of publication: Corey, Joyce Y.; Trankler, Kevin A.; Braddock-Wilking, Janet; Rath, Nigam P.
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 21
• Pages of publication: 5708
• a: 19.7846 ± 0.0004 Å
• b: 21.0568 ± 0.0004 Å
• c: 25.5326 ± 0.0005 Å
• α: 90°
• β: 93.966 ± 0.001°
• γ: 90°
• Cell volume: 10611.4 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 3
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1168
• Residual factor for significantly intense reflections: 0.0604
• Weighted residual factors for significantly intense reflections: 0.1359
• Weighted residual factors for all reflections included in the refinement: 0.159
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No