Information card for entry 4066677

Structure parameters

• Formula: C103 H129 N6 S4 Si2
• Calculated formula: C103 H129 N6 S4 Si2
• Title of publication: Synthesis and Reactivity of a Base-Free N-Heterocyclic Silanimine†
• Authors of publication: Kong, Lingbing; Cui, Chunming
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 22
• Pages of publication: 5738
• a: 10.9167 ± 0.0019 Å
• b: 19.022 ± 0.003 Å
• c: 23.425 ± 0.003 Å
• α: 89.86 ± 0.013°
• β: 83.91 ± 0.009°
• γ: 74.496 ± 0.012°
• Cell volume: 4659.2 ± 1.3 ų
• Cell temperature: 113 ± 2 K
• Ambient diffraction temperature: 113 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0705
• Residual factor for significantly intense reflections: 0.0558
• Weighted residual factors for significantly intense reflections: 0.1383
• Weighted residual factors for all reflections included in the refinement: 0.147
• Goodness-of-fit parameter for all reflections included in the refinement: 1.088
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No