Information card for entry 4066783

Structure parameters

• Formula: C18 H36 P2 Pd Si2
• Calculated formula: C18 H36 P2 Pd Si2
• SMILES: [Pd]12([P](CC[P]1(CC)CC)(CC)CC)[Si](c1ccccc1[SiH2]2)(C)C
• Title of publication: Ligand-Dependent Selective Formation of Unique Silylpalladium Complexes by the Reaction of 1-(Dimethylsilyl)-2-silylbenzene and [{1,2-C6H4(SiMe2)(SiH2)}Pd(R2PCH2CH2PR2)]
• Authors of publication: Li, Yong-Hua; Shimada, Shigeru
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 19
• Pages of publication: 4406
• a: 9.3937 ± 0.0005 Å
• b: 13.7246 ± 0.0007 Å
• c: 18.2952 ± 0.0009 Å
• α: 90°
• β: 104.44 ± 0.001°
• γ: 90°
• Cell volume: 2284.2 ± 0.2 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.0255
• Weighted residual factors for all reflections included in the refinement: 0.0575
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No