Information card for entry 4066785

Structure parameters

• Formula: C44 H74 P4 Pd2 Si8
• Calculated formula: C44 H64.4 P4 Pd2 Si8
• Title of publication: Ligand-Dependent Selective Formation of Unique Silylpalladium Complexes by the Reaction of 1-(Dimethylsilyl)-2-silylbenzene and [{1,2-C6H4(SiMe2)(SiH2)}Pd(R2PCH2CH2PR2)]
• Authors of publication: Li, Yong-Hua; Shimada, Shigeru
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 19
• Pages of publication: 4406
• a: 21.2824 ± 0.0011 Å
• b: 15.072 ± 0.0007 Å
• c: 18.9467 ± 0.001 Å
• α: 90°
• β: 111.237 ± 0.001°
• γ: 90°
• Cell volume: 5664.8 ± 0.5 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for significantly intense reflections: 0.032
• Weighted residual factors for all reflections included in the refinement: 0.0708
• Goodness-of-fit parameter for all reflections included in the refinement: 0.986
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No