Information card for entry 4066805

Structure parameters

• Formula: C73 H78 Cl6 N6 Ni Pt
• Calculated formula: C73 H78 Cl6 N6 Ni Pt
• Title of publication: Platinum(II) and Platinum(IV) Porphyrin Pincer Complexes: Synthesis, Structures, and Reactivity
• Authors of publication: Yoshida, Keita; Yamaguchi, Shigeru; Osuka, Atsuhiro; Shinokubo, Hiroshi
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 17
• Pages of publication: 3997
• a: 42.745 ± 0.005 Å
• b: 14.683 ± 0.005 Å
• c: 27.725 ± 0.005 Å
• α: 90 ± 0.005°
• β: 125.799 ± 0.005°
• γ: 90 ± 0.005°
• Cell volume: 14113 ± 6 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0636
• Residual factor for significantly intense reflections: 0.0519
• Weighted residual factors for significantly intense reflections: 0.1428
• Weighted residual factors for all reflections included in the refinement: 0.1491
• Goodness-of-fit parameter for all reflections included in the refinement: 0.992
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No