Information card for entry 4066841

Structure parameters

• Formula: C42 H59 Mg N3 O Si
• Calculated formula: C42 H59 Mg N3 O Si
• Title of publication: Intramolecular Aminoalkene Hydroamination Catalyzed by Magnesium Complexes Containing Multidentate Phenoxyamine Ligands
• Authors of publication: Zhang, Xiaoming; Emge, Thomas J.; Hultzsch, Kai C.
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 22
• Pages of publication: 5871
• a: 10.7798 ± 0.0007 Å
• b: 14.4804 ± 0.0009 Å
• c: 25.3779 ± 0.0015 Å
• α: 90°
• β: 94.55 ± 0.001°
• γ: 90°
• Cell volume: 3948.9 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0711
• Residual factor for significantly intense reflections: 0.0518
• Weighted residual factors for significantly intense reflections: 0.1159
• Weighted residual factors for all reflections included in the refinement: 0.1236
• Goodness-of-fit parameter for all reflections included in the refinement: 1.008
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No