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Information card for entry 4066910
Preview
Coordinates | 4066910.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C30 H28 Cl2 F3 I2 O P2 Rh |
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Calculated formula | C30 H28 Cl2 F3 I2 O P2 Rh |
SMILES | I[Rh]1(I)([P](CCC[P]1(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1)C(=O)C(F)(F)F.ClCCl |
Title of publication | Comparison of the Thermal and Reductive Decarbonylation of a Rhodium Trifluoroacetyl Diphosphine Complex |
Authors of publication | Panthi, Basu D.; Gipson, Stephen L.; Franken, Andreas |
Journal of publication | Organometallics |
Year of publication | 2010 |
Journal volume | 29 |
Journal issue | 22 |
Pages of publication | 5890 |
a | 9.5 ± 0.002 Å |
b | 13.385 ± 0.004 Å |
c | 14.187 ± 0.004 Å |
α | 74.522 ± 0.014° |
β | 79.145 ± 0.012° |
γ | 70.165 ± 0.012° |
Cell volume | 1625.9 ± 0.8 Å3 |
Cell temperature | 110 ± 2 K |
Ambient diffraction temperature | 110 ± 2 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0266 |
Residual factor for significantly intense reflections | 0.0223 |
Weighted residual factors for significantly intense reflections | 0.048 |
Weighted residual factors for all reflections included in the refinement | 0.0505 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.04 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4066910.html
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