Information card for entry 4066926

Structure parameters

• Formula: C26 H55 F6 N2 O2.5 Os P2 Si
• Calculated formula: C26 H55 F6 N2 O2.5 Os P2 Si
• Title of publication: Efficient Concatenation of C═C Reduction, C−H Bond Activation, and C−C and C−N Coupling Reactions on Osmium: Assembly of Two Allylamines and an Allene
• Authors of publication: Baya, Miguel; Esteruelas, Miguel A.; Oñate, Enrique
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 23
• Pages of publication: 6298
• a: 14.676 ± 0.005 Å
• b: 15.476 ± 0.005 Å
• c: 16.336 ± 0.005 Å
• α: 90°
• β: 109.164 ± 0.005°
• γ: 90°
• Cell volume: 3505 ± 2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0903
• Residual factor for significantly intense reflections: 0.0554
• Weighted residual factors for significantly intense reflections: 0.0931
• Weighted residual factors for all reflections included in the refinement: 0.1022
• Goodness-of-fit parameter for all reflections included in the refinement: 1.077
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No