Information card for entry 4066955

Structure parameters

• Formula: C14 H6 Fe Mn O8 P
• Calculated formula: C14 H6 Fe Mn O8 P
• Title of publication: Synthesis, Characterization, and Reactivity of the Heterometallic Dinuclear μ-PH2and μ-PPhH Complexes FeMn(CO)8(μ-PH2) and FeMn(CO)8(μ-PPhH)‡
• Authors of publication: Colson, Adam C.; Whitmire, Kenton H.
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 20
• Pages of publication: 4611
• a: 10.242 ± 0.004 Å
• b: 14.193 ± 0.006 Å
• c: 11.935 ± 0.005 Å
• α: 90°
• β: 97.927 ± 0.008°
• γ: 90°
• Cell volume: 1718.3 ± 1.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.2164
• Residual factor for significantly intense reflections: 0.0775
• Weighted residual factors for significantly intense reflections: 0.1328
• Weighted residual factors for all reflections included in the refinement: 0.1676
• Goodness-of-fit parameter for all reflections included in the refinement: 1.122
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No