Information card for entry 4066961

Structure parameters

• Formula: C57 H73 Cl2 N3 Si
• Calculated formula: C57 H73 Cl2 N3 Si
• Title of publication: N-Heterocyclic Carbene Stabilized Dichlorosilaimine IPr·Cl2Si═NR
• Authors of publication: Ghadwal, Rajendra S.; Roesky, Herbert W.; Schulzke, Carola; Granitzka, Markus
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 23
• Pages of publication: 6329
• a: 18.674 ± 0.003 Å
• b: 14.193 ± 0.002 Å
• c: 38.194 ± 0.006 Å
• α: 90°
• β: 93.331 ± 0.002°
• γ: 90°
• Cell volume: 10106 ± 3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0758
• Residual factor for significantly intense reflections: 0.0475
• Weighted residual factors for significantly intense reflections: 0.1026
• Weighted residual factors for all reflections included in the refinement: 0.1163
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No