Information card for entry 4067012

Structure parameters

• Formula: C50.5 H63 B Cl3 N Ru2 S
• Calculated formula: C50.5 H62 B Cl3 N Ru2 S
• Title of publication: Synthesis and Reactivity of 2-Aminoethanethiolato-Bridged Dinuclear Ru(hmb) Complexes (hmb = η6-hexamethylbenzene): Mechanistic Consideration on Transfer Hydrogenation with Bifunctional [RuCl2(hmb)]2/2-Aminoethanethiol Catalyst System
• Authors of publication: Ito, Masato; Watanabe, Akira; Shibata, Yuji; Ikariya, Takao
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 20
• Pages of publication: 4584
• a: 21.752 ± 0.009 Å
• b: 14.934 ± 0.006 Å
• c: 29.315 ± 0.012 Å
• α: 90°
• β: 100.981 ± 0.005°
• γ: 90°
• Cell volume: 9348 ± 7 ų
• Cell temperature: 193.1 K
• Ambient diffraction temperature: 193.1 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.0499
• Weighted residual factors for all reflections included in the refinement: 0.1727
• Goodness-of-fit parameter for all reflections included in the refinement: 1.002
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No