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Information card for entry 4067169
Preview
Coordinates | 4067169.cif |
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Original paper (by DOI) | HTML |
Chemical name | Trimethyl(2,3,5-triphenyl-1,3-pentadien-5-one)phosphonium perchlorate |
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Formula | C26 H26 Cl O5 P |
Calculated formula | C26 H26 Cl O5 P |
Title of publication | Unprecedented Ring Transformation of an α,α′-Monosubstituted 2,4,5-Triphenylpyrylium Salt with η3-Phosphines: Efficient Synthesis of Aryl- and Alkylphosphonium Triphenylcyclopentadienylides |
Authors of publication | Xu, Tao; Gong, Wei-tao; Ye, Jun-wei; Lin, Yuan; Ning, Gui-ling |
Journal of publication | Organometallics |
Year of publication | 2010 |
Journal volume | 29 |
Journal issue | 24 |
Pages of publication | 6744 |
a | 10.6802 ± 0.0005 Å |
b | 22.1133 ± 0.001 Å |
c | 11.5904 ± 0.0005 Å |
α | 90° |
β | 114.767 ± 0.003° |
γ | 90° |
Cell volume | 2485.6 ± 0.2 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.1128 |
Residual factor for significantly intense reflections | 0.0736 |
Weighted residual factors for significantly intense reflections | 0.2385 |
Weighted residual factors for all reflections included in the refinement | 0.2833 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.998 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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