Information card for entry 4067172

Structure parameters

• Formula: C34.25 H49 O2 S2 Si2 W
• Calculated formula: C34.25 H46 O2 S2 Si2 W
• Title of publication: Reactions of (Silyl)(silylene)tungsten and -molybdenum Complexes with Sulfur Reagents
• Authors of publication: Muraoka, Takako; Nakamura, Tomoko; Nakamura, Atsushi; Ueno, Keiji
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 24
• Pages of publication: 6624
• a: 11.566 ± 0.003 Å
• b: 11.7367 ± 0.0011 Å
• c: 16.033 ± 0.003 Å
• α: 71.64 ± 0.04°
• β: 83.42 ± 0.05°
• γ: 63.19 ± 0.04°
• Cell volume: 1842.6 ± 1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0362
• Residual factor for significantly intense reflections: 0.0353
• Weighted residual factors for significantly intense reflections: 0.0856
• Weighted residual factors for all reflections included in the refinement: 0.0868
• Goodness-of-fit parameter for all reflections included in the refinement: 1.341
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No