Information card for entry 4067189

Structure parameters

• Formula: C32 H44 Fe2 N2 Si4
• Calculated formula: C32 H44 Fe2 N2 Si4
• SMILES: [Fe]123456([Si](c7c([Si]1(C)C)cccc7)(C)C)([N]#[N][Fe]1789%10%11([Si](c%12c([Si]1(C)C)cccc%12)(C)C)[cH]1[cH]7[cH]8[cH]9[cH]%10[cH]%111)[cH]1[cH]2[cH]3[cH]4[cH]5[cH]61
• Title of publication: Half-Sandwich (η6-Arene)iron(II) Dinitrogen Complexes Bearing a Disilaferracycle Skeleton as a Precursor for Double Silylation of Ethylene and Alkynes
• Authors of publication: Sunada, Yusuke; Imaoka, Tsuyoshi; Nagashima, Hideo
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 23
• Pages of publication: 6157
• a: 10.1135 ± 0.0019 Å
• b: 11.476 ± 0.002 Å
• c: 15.057 ± 0.003 Å
• α: 108.982 ± 0.003°
• β: 90.155 ± 0.002°
• γ: 97.604 ± 0.002°
• Cell volume: 1636 ± 0.5 ų
• Cell temperature: 123.1 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0484
• Weighted residual factors for all reflections included in the refinement: 0.1475
• Goodness-of-fit parameter for all reflections included in the refinement: 1.512
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No