Information card for entry 4067297

Structure parameters

• Chemical name: bis(3-methylpyridine)-bis(s-butyl)-zinc toluene clathrate
• Formula: C27 H32 N2 Zn
• Calculated formula: C27 H32 N2 Zn
• Title of publication: Toward Total Spontaneous Resolution ofsec-Butylzinc Complexes
• Authors of publication: Lennartson, Anders; Hedström, Anna; Håkansson, Mikael
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 1
• Pages of publication: 177
• a: 10.787 ± 0.007 Å
• b: 11.093 ± 0.008 Å
• c: 11.889 ± 0.002 Å
• α: 71.019 ± 0.012°
• β: 72.879 ± 0.013°
• γ: 85.313 ± 0.016°
• Cell volume: 1285.5 ± 1.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0512
• Residual factor for significantly intense reflections: 0.0498
• Weighted residual factors for significantly intense reflections: 0.1308
• Weighted residual factors for all reflections included in the refinement: 0.1316
• Goodness-of-fit parameter for all reflections included in the refinement: 1.089
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No