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Information card for entry 4067308
Preview
Coordinates | 4067308.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C43 H44 Cl N O5 P2 Pd |
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Calculated formula | C43 H44 Cl N O5 P2 Pd |
SMILES | [Pd]12(c3ccc4c(cccc4)c3[C@@H](C)[N]1(C)C)[P](c1ccccc1)(c1ccccc1)[C@H](C[P]2(c1ccccc1)c1ccccc1)CC(=O)C.Cl(=O)(=O)(=O)[O-] |
Title of publication | Palladium Template Promoted Asymmetric Synthesis of 1,2-Diphosphines by Hydrophosphination of Functionalized Allenes |
Authors of publication | Huang, Yinhua; Pullarkat, Sumod A.; Yuan, Mingjun; Ding, Yi; Li, Yongxin; Leung, Pak-Hing |
Journal of publication | Organometallics |
Year of publication | 2010 |
Journal volume | 29 |
Journal issue | 3 |
Pages of publication | 536 |
a | 11.9241 ± 0.0002 Å |
b | 15.8526 ± 0.0003 Å |
c | 21.0733 ± 0.0004 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 3983.44 ± 0.13 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 7 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0378 |
Residual factor for significantly intense reflections | 0.0306 |
Weighted residual factors for significantly intense reflections | 0.09 |
Weighted residual factors for all reflections included in the refinement | 0.1112 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.146 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4067308.html
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