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Information card for entry 4067311
Preview
Coordinates | 4067311.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C29 H31 B F4 N4 O2 Pd2 |
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Calculated formula | C29 H31 B F4 N4 O2 Pd2 |
Title of publication | Dinuclear Allylpalladium Complexes ofC2-Symmetric Pyrazolate-Bridged Bis(oxazoline) Ligands (pyrbox's): Structures, Dynamic Behavior, and Application in Asymmetric Allylic Alkylation |
Authors of publication | Ficks, Arne; Sibbald, Connor; John, Michael; Dechert, Sebastian; Meyer, Franc |
Journal of publication | Organometallics |
Year of publication | 2010 |
Journal volume | 29 |
Journal issue | 5 |
Pages of publication | 1117 |
a | 13.5487 ± 0.0004 Å |
b | 13.5487 ± 0.0004 Å |
c | 27.8944 ± 0.001 Å |
α | 90° |
β | 90° |
γ | 120° |
Cell volume | 4434.5 ± 0.2 Å3 |
Cell temperature | 133 ± 2 K |
Ambient diffraction temperature | 133 ± 2 K |
Number of distinct elements | 7 |
Space group number | 169 |
Hermann-Mauguin space group symbol | P 61 |
Hall space group symbol | P 61 |
Residual factor for all reflections | 0.0566 |
Residual factor for significantly intense reflections | 0.0547 |
Weighted residual factors for significantly intense reflections | 0.1244 |
Weighted residual factors for all reflections included in the refinement | 0.1256 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.065 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4067311.html
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