Use of73Ge NMR Spectroscopy and X-ray Crystallography for the Study of Electronic Interactions in Substituted Tetrakis(phenyl)-, -(phenoxy)-, and -(thiophenoxy)germanes
Authors of publication
Yoder, Claude H.; Agee, Tamara M.; Griffith, Allison K.; Schaeffer, Charles D.; Carroll, Mary J.; DeToma, Alaina S.; Fleisher, Adam J.; Gettel, Cameron J.; Rheingold, Arnold L.
Journal of publication
Organometallics
Year of publication
2010
Journal volume
29
Journal issue
3
Pages of publication
582
a
8.5326 ± 0.0009 Å
b
8.8304 ± 0.0009 Å
c
16.6832 ± 0.0016 Å
α
80.629 ± 0.001°
β
82.178 ± 0.001°
γ
89.63 ± 0.001°
Cell volume
1228.5 ± 0.2 Å3
Cell temperature
208 ± 2 K
Ambient diffraction temperature
208 ± 2 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0535
Residual factor for significantly intense reflections
0.0361
Weighted residual factors for significantly intense reflections
0.0806
Weighted residual factors for all reflections included in the refinement
0.089
Goodness-of-fit parameter for all reflections included in the refinement
