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Information card for entry 4067404
Preview
Coordinates | 4067404.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C37 H31 Cl5 N2 P2 Pd |
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Calculated formula | C37 H31 Cl5 N2 P2 Pd |
SMILES | C(Cl)(Cl)Cl.c1(ccccc1)[P]1(c2ccccc2)N(c2ccccc2)N(c2ccccc2)[P](c2ccccc2)(c2ccccc2)[Pd]1(Cl)Cl |
Title of publication | Synthesis, Coordination Chemistry, and Catalysis of the First 1,2-Bis(diphenylphosphino)-1,2-diphenylhydrazine, Ph2PN(Ph)N(Ph)PPh2† |
Authors of publication | Aluri, Bhaskar R.; Peulecke, Normen; Müller, Bernd H.; Peitz, Stephan; Spannenberg, Anke; Hapke, Marko; Rosenthal, Uwe |
Journal of publication | Organometallics |
Year of publication | 2010 |
Journal volume | 29 |
Journal issue | 1 |
Pages of publication | 226 |
a | 9.34584 ± 0.00018 Å |
b | 18.8018 ± 0.0003 Å |
c | 21.4718 ± 0.0004 Å |
α | 90° |
β | 93.5968 ± 0.0016° |
γ | 90° |
Cell volume | 3765.56 ± 0.12 Å3 |
Cell temperature | 200 ± 2 K |
Ambient diffraction temperature | 200 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0325 |
Residual factor for significantly intense reflections | 0.0236 |
Weighted residual factors for significantly intense reflections | 0.0572 |
Weighted residual factors for all reflections included in the refinement | 0.0587 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.964 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4067404.html
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