Information card for entry 4067427

Structure parameters

• Formula: C37.5 H52 B2 Cl F8 N7 Os
• Calculated formula: C37.5 H52 B2 Cl F8 N7 Os
• Title of publication: Dicationic Alkylidene−, Olefin−, and Alkoxyalkenylcarbene−Osmium Complexes Stabilized by a NHC Ligand
• Authors of publication: Buil, María L.; Castarlenas, Ricardo; Esteruelas, Miguel A.; Izquierdo, Susana; Lalrempuia, Ralte; Oñate, Enrique
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 4
• Pages of publication: 876
• a: 12.0654 ± 0.0019 Å
• b: 12.944 ± 0.002 Å
• c: 31.086 ± 0.005 Å
• α: 90°
• β: 100.657 ± 0.003°
• γ: 90°
• Cell volume: 4771.1 ± 1.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1051
• Residual factor for significantly intense reflections: 0.0634
• Weighted residual factors for significantly intense reflections: 0.161
• Weighted residual factors for all reflections included in the refinement: 0.1856
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No