Information card for entry 4067435

Structure parameters

• Formula: C66.5 H53 Cl P2 Si
• Calculated formula: C66.5 H53 Cl P2 Si
• Title of publication: Preparation and Photophysical Properties of Phosphino- and Phosphine Oxide-Linked Siloles
• Authors of publication: Braddock-Wilking, Janet; Gao, Li-Bin; Rath, Nigam P.
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 7
• Pages of publication: 1612
• a: 46.444 ± 0.008 Å
• b: 9.5894 ± 0.0018 Å
• c: 24.803 ± 0.005 Å
• α: 90°
• β: 106.484 ± 0.015°
• γ: 90°
• Cell volume: 10592 ± 4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.2647
• Residual factor for significantly intense reflections: 0.0993
• Weighted residual factors for significantly intense reflections: 0.2524
• Weighted residual factors for all reflections included in the refinement: 0.3571
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No