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Information card for entry 4067452
Preview
Coordinates | 4067452.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C52 H34 Cl6 O20 Os6 P2 S2 |
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Calculated formula | C52 H34 Cl6 O20 Os6 P2 S2 |
Title of publication | Synthesis, Characterization, and Novel Fluxional Mechanisms of Triosmium Clusters Containing the Highly Flexible Ligand Ph2PC2H4SC2H4SC2H4PPh2(PSSP) |
Authors of publication | Persson, Roger; Stchedroff, Marc J.; Uebersezig, Bettina; Gobetto, Roberto; Steed, Jonathan W.; Prince, Paul D.; Monari, Magda; Nordlander, Ebbe |
Journal of publication | Organometallics |
Year of publication | 2010 |
Journal volume | 29 |
Journal issue | 10 |
Pages of publication | 2223 |
a | 13.9222 ± 0.0006 Å |
b | 15.5954 ± 0.0007 Å |
c | 17.5669 ± 0.0008 Å |
α | 109.624 ± 0.001° |
β | 99.645 ± 0.002° |
γ | 104.675 ± 0.002° |
Cell volume | 3339.2 ± 0.3 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1024 |
Residual factor for significantly intense reflections | 0.0471 |
Weighted residual factors for significantly intense reflections | 0.1002 |
Weighted residual factors for all reflections included in the refinement | 0.1143 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.901 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4067452.html
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