Information card for entry 4067500

Structure parameters

• Formula: C59.5 H62 Mg2 N2 P4 S2 Si2
• Calculated formula: C59.5 H58 Mg2 N2 P4 S2 Si2
• Title of publication: Synthesis and Characterization of Magnesium and Aluminum Bis(phosphoranyl)methanediide Complexes
• Authors of publication: Guo, Jiayi; Lee, Jia-Shin; Foo, Ming-Choo; Lau, Kai-Chung; Xi, Hong-Wei; Lim, Kok Hwa; So, Cheuk-Wai
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 4
• Pages of publication: 939
• a: 13.4186 ± 0.0004 Å
• b: 24.1503 ± 0.0006 Å
• c: 19.3995 ± 0.0005 Å
• α: 90°
• β: 107.751 ± 0.002°
• γ: 90°
• Cell volume: 5987.4 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0857
• Residual factor for significantly intense reflections: 0.0526
• Weighted residual factors for significantly intense reflections: 0.1394
• Weighted residual factors for all reflections included in the refinement: 0.1937
• Goodness-of-fit parameter for all reflections included in the refinement: 1.173
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No