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Information card for entry 4067606
Preview
Coordinates | 4067606.cif |
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Original paper (by DOI) | HTML |
Formula | C38 H62 N2 Os P2 |
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Calculated formula | C38 H62 N2 Os P2 |
Title of publication | Multiple C−H Bond Activation of Phenyl-Substituted Pyrimidines and Triazines Promoted by an Osmium Polyhydride: Formation of Osmapolycycles with Three, Five, and Eight Fused Rings |
Authors of publication | Esteruelas, Miguel A.; Fernández, Israel; Herrera, Antonio; Martín-Ortiz, Mamen; Martínez-Álvarez, Roberto; Oliván, Montserrat; Oñate, Enrique; Sierra, Miguel A.; Valencia, Marta |
Journal of publication | Organometallics |
Year of publication | 2010 |
Journal volume | 29 |
Journal issue | 4 |
Pages of publication | 976 |
a | 10.724 ± 0.003 Å |
b | 11.504 ± 0.003 Å |
c | 15.107 ± 0.004 Å |
α | 88.454 ± 0.004° |
β | 77.692 ± 0.004° |
γ | 82.541 ± 0.005° |
Cell volume | 1805.5 ± 0.8 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0567 |
Residual factor for significantly intense reflections | 0.0439 |
Weighted residual factors for significantly intense reflections | 0.0852 |
Weighted residual factors for all reflections included in the refinement | 0.0891 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.963 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4067606.html
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Users of the data should acknowledge the original authors of the
structural data.