Information card for entry 4067621

Structure parameters

• Chemical name: 2,6-bis[1,1-dihydroxy-2,2,2-trifluoroethyl]pyridine
• Formula: C13 H15 F6 N O5
• Calculated formula: C13 H15 F6 N O5
• Title of publication: (Py)2Co(CH2SiMe3)2As an Easily Accessible Source of “CoR2”
• Authors of publication: Zhu, Di; Janssen, Femke F. B. J.; Budzelaar, Peter H. M.
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 8
• Pages of publication: 1897
• a: 6.6689 ± 0.0003 Å
• b: 14.6578 ± 0.0008 Å
• c: 17.1651 ± 0.0012 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1677.91 ± 0.17 ų
• Cell temperature: 208 ± 2 K
• Ambient diffraction temperature: 208 ± 2 K
• Number of distinct elements: 5
• Space group number: 62
• Hermann-Mauguin space group symbol: P c m n
• Hall space group symbol: -P 2n 2ac
• Residual factor for all reflections: 0.0916
• Residual factor for significantly intense reflections: 0.0623
• Weighted residual factors for all reflections: 0.1446
• Weighted residual factors for significantly intense reflections: 0.1326
• Weighted residual factors for all reflections included in the refinement: 0.1446
• Goodness-of-fit parameter for all reflections: 1.086
• Goodness-of-fit parameter for all reflections included in the refinement: 1.086
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No