Crystallography Open Database

Information card for entry 4067630

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Coordinates	4067630.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C44 H69 Al P2
Calculated formula	C44 H69 Al P2
Title of publication	C≡C Triple Bond Activation by Heterocyclic Aluminum Phosphinides
Authors of publication	Westenberg, Hauke; Slootweg, J. Chris; Hepp, Alexander; Kösters, Jutta; Roters, Steffi; Ehlers, Andreas W.; Lammertsma, Koop; Uhl, Werner
Journal of publication	Organometallics
Year of publication	2010
Journal volume	29
Journal issue	6
Pages of publication	1323
a	23.453 ± 0.005 Å
b	18.823 ± 0.004 Å
c	22.344 ± 0.005 Å
α	90°
β	114.66 ± 0.03°
γ	90°
Cell volume	8964 ± 4 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.2189
Residual factor for significantly intense reflections	0.0507
Weighted residual factors for significantly intense reflections	0.0632
Weighted residual factors for all reflections included in the refinement	0.0863
Goodness-of-fit parameter for all reflections included in the refinement	0.554
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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