Information card for entry 4067639

Structure parameters

• Formula: C26 H72 Si11
• Calculated formula: C26 H72 Si11
• Title of publication: Synthesis and Facile Ring Expansion of Silylenecyclotetrasilane
• Authors of publication: Iwamoto, Takeaki; Furiya, Yuichi; Kobayashi, Hideki; Isobe, Hiroyuki; Kira, Mitsuo
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 8
• Pages of publication: 1869
• a: 13.572 ± 0.0019 Å
• b: 18.57 ± 0.003 Å
• c: 17.526 ± 0.002 Å
• α: 90°
• β: 92.864 ± 0.002°
• γ: 90°
• Cell volume: 4411.6 ± 1.1 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 3
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0452
• Residual factor for significantly intense reflections: 0.0317
• Weighted residual factors for significantly intense reflections: 0.0745
• Weighted residual factors for all reflections included in the refinement: 0.0831
• Goodness-of-fit parameter for all reflections included in the refinement: 1.082
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No