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Information card for entry 4067740
Preview
Coordinates | 4067740.cif |
---|---|
Original paper (by DOI) | HTML |
External links | ChemSpider |
Formula | C27 H27 N P2 S2 |
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Calculated formula | C27 H27 N P2 S2 |
SMILES | c1(ccccc1)P(c1ccccc1)(CN(CP(c1ccccc1)(c1ccccc1)=S)C)=S |
Title of publication | Reactivity of [Fe2(CO)6(μ-S2)] toward a Base-Containing Diphosphine (Ph2PCH2)2NCH3: Formation of Diiron Carbonyl Compounds Having Polydentate Heterofunctionalized Phosphine (PNS = Ph2PCH2N(CH3)CH2S) and Bidentate Thiophosphinito (Ph2PS = PS) Bridges |
Authors of publication | Lounissi, Sondès; Capon, Jean-François; Gloaguen, Frédéric; Matoussi, Fatma; Pétillon, François Y.; Schollhammer, Philippe; Talarmin, Jean |
Journal of publication | Organometallics |
Year of publication | 2010 |
Journal volume | 29 |
Journal issue | 5 |
Pages of publication | 1296 |
a | 15.3111 ± 0.0008 Å |
b | 7.7994 ± 0.0004 Å |
c | 21.3862 ± 0.0012 Å |
α | 90° |
β | 103.533 ± 0.006° |
γ | 90° |
Cell volume | 2483 ± 0.2 Å3 |
Cell temperature | 170 ± 2 K |
Ambient diffraction temperature | 170 ± 2 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0784 |
Residual factor for significantly intense reflections | 0.0427 |
Weighted residual factors for significantly intense reflections | 0.104 |
Weighted residual factors for all reflections included in the refinement | 0.1168 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.967 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4067740.html
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