Information card for entry 4067795

Structure parameters

• Formula: C41 H41 Co O8
• Calculated formula: C41 H41 Co O8
• Title of publication: An Improved Protocol for the Synthesis of [(η4-C4R4)Co(η5-C5H5)] Complexes
• Authors of publication: Bertrand, Guillaume; Tortech, Ludovic; Fichou, Denis; Malacria, Max; Aubert, Corinne; Gandon, Vincent
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 1
• Pages of publication: 126
• a: 15.6941 ± 0.0004 Å
• b: 15.6941 ± 0.0004 Å
• c: 7.2842 ± 0.0002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1794.13 ± 0.08 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 4
• Space group number: 104
• Hermann-Mauguin space group symbol: P 4 n c
• Hall space group symbol: P 4 -2n
• Residual factor for all reflections: 0.0419
• Residual factor for significantly intense reflections: 0.035
• Weighted residual factors for significantly intense reflections: 0.0884
• Weighted residual factors for all reflections included in the refinement: 0.0919
• Goodness-of-fit parameter for all reflections included in the refinement: 1.146
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No