Crystallography Open Database

Information card for entry 4067934

Preview

Coordinates	4067934.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C27 H43 F6 N3 O6 P3 Ru S2 Si
Calculated formula	C26.5 H42.99 F4.5 N3 O4.5 P3 Ru S1.5 Si
Title of publication	Asymmetric Synthesis and Metal Complexes of aC3-Symmetric P-Stereogenic Triphosphine, (R)-MeSi(CH2PMe(t-Bu))3(MT-Siliphos)
Authors of publication	Cain, Matthew F.; Glueck, David S.; Golen, James A.; Rheingold, Arnold L.
Journal of publication	Organometallics
Year of publication	2012
Journal volume	31
Journal issue	3
Pages of publication	775
a	25.5296 ± 0.0015 Å
b	25.5296 ± 0.0015 Å
c	25.5296 ± 0.0015 Å
α	90°
β	90°
γ	90°
Cell volume	16639.2 ± 1.7 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	9
Space group number	198
Hermann-Mauguin space group symbol	P 21 3
Hall space group symbol	P 2ac 2ab 3
Residual factor for all reflections	0.0709
Residual factor for significantly intense reflections	0.0603
Weighted residual factors for significantly intense reflections	0.1475
Weighted residual factors for all reflections included in the refinement	0.1535
Goodness-of-fit parameter for all reflections included in the refinement	1.001
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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