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Information card for entry 4068076
Preview
Coordinates | 4068076.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C23 H38 F6 Os P2 |
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Calculated formula | C23 H38 F6 Os P2 |
SMILES | [Os]12345678([P](C4(C[C]2(C1)=[CH]3C1CCCCC1)C)(C(C)C)C(C)C)[cH]1[cH]5[cH]6[cH]7[cH]81.[P](F)(F)(F)(F)(F)[F-] |
Title of publication | Formation of Osmium-Allylphosphinomethanide Complexes by Coupling of an Isopropenyldiisopropylphosphine and Monosubstituted Allenes |
Authors of publication | Esteruelas, Miguel A.; López, Ana M.; Mozo, Silvia; Oñate, Enrique |
Journal of publication | Organometallics |
Year of publication | 2012 |
Journal volume | 31 |
Journal issue | 1 |
Pages of publication | 440 |
a | 17.5094 ± 0.0002 Å |
b | 15.9826 ± 0.0002 Å |
c | 18.311 ± 0.0002 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 5124.26 ± 0.1 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 5 |
Space group number | 61 |
Hermann-Mauguin space group symbol | P b c a |
Hall space group symbol | -P 2ac 2ab |
Residual factor for all reflections | 0.0786 |
Residual factor for significantly intense reflections | 0.0351 |
Weighted residual factors for significantly intense reflections | 0.0781 |
Weighted residual factors for all reflections included in the refinement | 0.0836 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.981 |
Diffraction radiation wavelength | 0.7107 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4068076.html
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Users of the data should acknowledge the original authors of the
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