Information card for entry 4068083

Structure parameters

• Formula: C30 H70 Cl4 Li2 Mg2 O6 Si4
• Calculated formula: C30 H70 Cl4 Li2 Mg2 O6 Si4
• Title of publication: An Approach to Pin Down the Solid-State Structure of the “Turbo Grignard”
• Authors of publication: Blasberg, Florian; Bolte, Michael; Wagner, Matthias; Lerner, Hans-Wolfram
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 3
• Pages of publication: 1001
• a: 19.139 ± 0.002 Å
• b: 15.126 ± 0.002 Å
• c: 16.9129 ± 0.0016 Å
• α: 90°
• β: 93.438 ± 0.008°
• γ: 90°
• Cell volume: 4887.4 ± 0.9 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1009
• Residual factor for significantly intense reflections: 0.0565
• Weighted residual factors for significantly intense reflections: 0.1199
• Weighted residual factors for all reflections included in the refinement: 0.1364
• Goodness-of-fit parameter for all reflections included in the refinement: 0.962
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No