Information card for entry 4068100

Structure parameters

• Formula: C48 H84 Cl4 N2 O3 P2 Pd2
• Calculated formula: C48 H84 Cl4 N2 O3 P2 Pd2
• Title of publication: Nickel and Palladium Complexes with New Phosphinito-Imine Ligands and Their Application as Ethylene Oligomerization Catalysts
• Authors of publication: Ortiz de la Tabla, Laura; Matas, Inmaculada; Palma, Pilar; Álvarez, Eleuterio; Cámpora, Juan
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 3
• Pages of publication: 1006
• a: 9.8987 ± 0.0014 Å
• b: 14.667 ± 0.002 Å
• c: 20.625 ± 0.003 Å
• α: 69.682 ± 0.004°
• β: 88.388 ± 0.005°
• γ: 77.26 ± 0.004°
• Cell volume: 2735.1 ± 0.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0319
• Residual factor for significantly intense reflections: 0.0253
• Weighted residual factors for significantly intense reflections: 0.0673
• Weighted residual factors for all reflections included in the refinement: 0.0692
• Goodness-of-fit parameter for all reflections included in the refinement: 1.08
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No