Information card for entry 4068288

Structure parameters

• Formula: C34 H60 N6 O0.5 Si
• Calculated formula: C34 H60 N6 O0.5 Si
• Title of publication: Synthesis and Reactivity of Three New N-Heterocyclic Silylenes
• Authors of publication: Tomasik, Adam C.; Mitra, Amitabha; West, Robert
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 1
• Pages of publication: 378
• a: 11.927 ± 0.008 Å
• b: 15.12 ± 0.011 Å
• c: 19.799 ± 0.011 Å
• α: 84.18 ± 0.03°
• β: 78.67 ± 0.04°
• γ: 74.32 ± 0.04°
• Cell volume: 3366 ± 4 ų
• Cell temperature: 103 ± 2 K
• Ambient diffraction temperature: 103 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0502
• Residual factor for significantly intense reflections: 0.044
• Weighted residual factors for significantly intense reflections: 0.1194
• Weighted residual factors for all reflections included in the refinement: 0.1244
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: Cu-Kα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No