Crystallography Open Database

Information card for entry 4068358

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Coordinates	4068358.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C48.75 H67 Au P
Calculated formula	C48.75 H67 Au P
Title of publication	Probing the Steric Limits of Carbon−Gold Bond Formation: (Dialkylbiarylphosphine)gold(I) Aryls
Authors of publication	Partyka, David V.; Updegraff, James B.; Zeller, Matthias; Hunter, Allen D.; Gray, Thomas G.
Journal of publication	Organometallics
Year of publication	2009
Journal volume	28
Journal issue	6
Pages of publication	1666
a	10.9277 ± 0.0004 Å
b	15.712 ± 0.0005 Å
c	25.4351 ± 0.0009 Å
α	76.644 ± 0.002°
β	87.555 ± 0.002°
γ	87.386 ± 0.002°
Cell volume	4242.3 ± 0.3 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0764
Residual factor for significantly intense reflections	0.0566
Weighted residual factors for significantly intense reflections	0.1486
Weighted residual factors for all reflections included in the refinement	0.1625
Goodness-of-fit parameter for all reflections included in the refinement	1.118
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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