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Information card for entry 4068390
Preview
Coordinates | 4068390.cif |
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Original paper (by DOI) | HTML |
Formula | C36 H62 N P2 V |
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Calculated formula | C36 H62 N P2 V |
SMILES | [V]12([P](c3cc(C)ccc3N1c1ccc(C)cc1[P]2(C(C)C)C(C)C)(C(C)C)C(C)C)(CC(C)(C)C)CC(C)(C)C |
Title of publication | A Transient Vanadium(III) Neopentylidene Complex. Redox Chemistry and Reactivity of the VCHtBu Functionality |
Authors of publication | Kilgore, Uriah J.; Sengelaub, Caitlin A.; Fan, Hongjun; Tomaszewski, John; Karty, Jonathan A.; Baik, Mu-Hyun; Mindiola, Daniel J. |
Journal of publication | Organometallics |
Year of publication | 2009 |
Journal volume | 28 |
Journal issue | 3 |
Pages of publication | 843 |
a | 18.661 ± 0.0009 Å |
b | 19.7507 ± 0.0009 Å |
c | 19.8391 ± 0.001 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 7312.1 ± 0.6 Å3 |
Cell temperature | 126 ± 2 K |
Ambient diffraction temperature | 126 ± 2 K |
Number of distinct elements | 5 |
Space group number | 61 |
Hermann-Mauguin space group symbol | P b c a |
Hall space group symbol | -P 2ac 2ab |
Residual factor for all reflections | 0.0543 |
Residual factor for significantly intense reflections | 0.0337 |
Weighted residual factors for significantly intense reflections | 0.0846 |
Weighted residual factors for all reflections included in the refinement | 0.0953 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.993 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4068390.html
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