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Information card for entry 4068396
Preview
Coordinates | 4068396.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C45 H40 B Cl N6 P2 Ru |
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Calculated formula | C45 H40 B Cl N6 P2 Ru |
Title of publication | Chlorination of Boron on a Ruthenium-Coordinated Hydridotris(pyrazolyl)borate (Tp) Ligand: A Caveat for the Use of TpRu(PPh3)2Cl |
Authors of publication | Foley, Nicholas A.; Abernethy, Robyn J.; Gunnoe, T. Brent; Hill, Anthony F.; Boyle, Paul D.; Sabat, Michal |
Journal of publication | Organometallics |
Year of publication | 2009 |
Journal volume | 28 |
Journal issue | 1 |
Pages of publication | 374 |
a | 17.6883 ± 0.0004 Å |
b | 12.2903 ± 0.0003 Å |
c | 18.8918 ± 0.0004 Å |
α | 90° |
β | 107.996 ± 0.0008° |
γ | 90° |
Cell volume | 3906.06 ± 0.16 Å3 |
Cell temperature | 110 K |
Ambient diffraction temperature | 110 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.047 |
Residual factor for significantly intense reflections | 0.038 |
Weighted residual factors for all reflections | 0.048 |
Weighted residual factors for all reflections included in the refinement | 0.048 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.37 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MolybdenumKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4068396.html
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