Information card for entry 4068506

Structure parameters

• Formula: C35 H49 Cl11 O Os P4
• Calculated formula: C35 H49 Cl11 O Os P4
• SMILES: O=C1[CH]2[Os]([P](C)(C)C)([P](C)(C)C)([P](C)(C)C)(Cl)([CH2]=2)C=C1[P+](c1ccccc1)(c1ccccc1)c1ccccc1.Cl.ClC(Cl)Cl.ClC(Cl)Cl.ClC(Cl)Cl
• Title of publication: Synthesis of Coordinated η2-α,β-Unsaturated Ketone Osmacycles from an Osmium-Coordinated Alkyne Alcohol Complex
• Authors of publication: Gong, Lei; Lin, Yumei; Wen, Ting Bin; Xia, Haiping
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 4
• Pages of publication: 1101
• a: 19.1611 ± 0.0016 Å
• b: 9.9137 ± 0.0008 Å
• c: 26.3 ± 0.002 Å
• α: 90°
• β: 105.754 ± 0.001°
• γ: 90°
• Cell volume: 4808.2 ± 0.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0549
• Residual factor for significantly intense reflections: 0.0298
• Weighted residual factors for significantly intense reflections: 0.0492
• Weighted residual factors for all reflections included in the refinement: 0.0527
• Goodness-of-fit parameter for all reflections included in the refinement: 1.001
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No