Novel Sterically Congested Monoorganobismuth(III) Compounds: Synthesis, Structure, and Bismuth−Arene π Interaction in ArBiXY (X, Y = Br, I, OH, 2,6-Mes2-4-t-Bu-C6H2PHO2)
Authors of publication
Breunig, Hans J.; Haddad, Nawja; Lork, Enno; Mehring, Michael; Mügge, Clemens; Nolde, Christof; Raţ, Ciprian I.; Schürmann, Markus
Journal of publication
Organometallics
Year of publication
2009
Journal volume
28
Journal issue
4
Pages of publication
1202
a
11.201 ± 0.002 Å
b
17.161 ± 0.004 Å
c
14.047 ± 0.003 Å
α
90°
β
95.25 ± 0.01°
γ
90°
Cell volume
2688.8 ± 1 Å3
Cell temperature
173 ± 2 K
Ambient diffraction temperature
173 ± 2 K
Number of distinct elements
4
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.1079
Residual factor for significantly intense reflections
0.0661
Weighted residual factors for significantly intense reflections
0.1585
Weighted residual factors for all reflections included in the refinement
0.181
Goodness-of-fit parameter for all reflections included in the refinement
