Information card for entry 4068597

Structure parameters

• Formula: C60 H59 F3 N2 O3 P3 Pt S
• Calculated formula: C60 H59 F3 N2 O3 P3 Pt S
• Title of publication: Phospha-Fischer Carbenes: Synthesis, Structure, Bonding, and Reactions of Pd(0)− and Pt(0)−Phosphenium Complexes
• Authors of publication: Caputo, Christine A.; Jennings, Michael C.; Tuononen, Heikki M.; Jones, Nathan D.
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 4
• Pages of publication: 990
• a: 12.8036 ± 0.0003 Å
• b: 13.6072 ± 0.0003 Å
• c: 16.6623 ± 0.0005 Å
• α: 76.956 ± 0.001°
• β: 75.841 ± 0.002°
• γ: 88.363 ± 0.002°
• Cell volume: 2741.02 ± 0.12 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0424
• Residual factor for significantly intense reflections: 0.0351
• Weighted residual factors for significantly intense reflections: 0.0799
• Weighted residual factors for all reflections included in the refinement: 0.083
• Goodness-of-fit parameter for all reflections included in the refinement: 1.073
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No