Information card for entry 4068705

Structure parameters

• Formula: C16 H29 Rh Si
• Calculated formula: C16 H29 Rh Si
• SMILES: [Rh]123456([c]7([c]1([c]2([c]3([c]47C)C)C)C)[Si](C)(C)C)([CH2]=[CH2]5)[CH2]=[CH2]6
• Title of publication: Zincocenes as Mild Cyclopentadienyl Transfer Reagents toward Rhodium(I) Olefin Precursors. Facile Synthesis of (η5-Cp′)Rh(olefin)2Compounds
• Authors of publication: Esqueda, Ana Cristina; Conejero, Salvador; Maya, Celia; Carmona, Ernesto
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 1
• Pages of publication: 45
• a: 7.0218 ± 0.0003 Å
• b: 8.7702 ± 0.0004 Å
• c: 15.3763 ± 0.0007 Å
• α: 78.226 ± 0.003°
• β: 82.215 ± 0.003°
• γ: 67.096 ± 0.002°
• Cell volume: 852.25 ± 0.07 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.048
• Residual factor for significantly intense reflections: 0.0379
• Weighted residual factors for significantly intense reflections: 0.1089
• Weighted residual factors for all reflections included in the refinement: 0.1434
• Goodness-of-fit parameter for all reflections included in the refinement: 1.077
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No