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Information card for entry 4068710
Preview
Coordinates | 4068710.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C36 H30 N2 O3 Si |
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Calculated formula | C36 H30 N2 O3 Si |
SMILES | [Si@@]123(Oc4ccccc4[C@@H](N2c2ccccc2[N]3=C(c2c(O1)cc(OC)cc2)c1ccccc1)CC=C)c1ccccc1.[Si@]123(Oc4ccccc4[C@H](N2c2ccccc2[N]3=C(c2c(O1)cc(OC)cc2)c1ccccc1)CC=C)c1ccccc1 |
Title of publication | Hypercoordinate Organosilicon Complexes of an ONN′O′ Chelating Ligand: Regio- and Diastereoselectivity of Rearrangement Reactions in Si−Salphen Systems |
Authors of publication | Lippe, Katrin; Gerlach, Daniela; Kroke, Edwin; Wagler, Jörg |
Journal of publication | Organometallics |
Year of publication | 2009 |
Journal volume | 28 |
Journal issue | 2 |
Pages of publication | 621 |
a | 16.5532 ± 0.0011 Å |
b | 14.9054 ± 0.0011 Å |
c | 22.7847 ± 0.0018 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 5621.7 ± 0.7 Å3 |
Cell temperature | 90 ± 2 K |
Ambient diffraction temperature | 90 ± 2 K |
Number of distinct elements | 5 |
Space group number | 61 |
Hermann-Mauguin space group symbol | P b c a |
Hall space group symbol | -P 2ac 2ab |
Residual factor for all reflections | 0.0813 |
Residual factor for significantly intense reflections | 0.0427 |
Weighted residual factors for significantly intense reflections | 0.0942 |
Weighted residual factors for all reflections included in the refinement | 0.1025 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.923 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4068710.html
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Users of the data should acknowledge the original authors of the
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