Information card for entry 4068781

Structure parameters

• Formula: C57.5 H51 Cl3 O3 Os P2
• Calculated formula: C57.5 H51 Cl3 O3 Os P2
• Title of publication: Nine-Membered Osmacycles Derived from Metathesis Reactions between Alkynes and an Osmafuran
• Authors of publication: Lin, Yumei; Gong, Lei; Xu, Hui; He, Xumin; Wen, Ting Bin; Xia, Haiping
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 5
• Pages of publication: 1524
• a: 13.3346 ± 0.0005 Å
• b: 13.6669 ± 0.0004 Å
• c: 16.7686 ± 0.0005 Å
• α: 104.013 ± 0.003°
• β: 105.535 ± 0.003°
• γ: 102.005 ± 0.003°
• Cell volume: 2732.29 ± 0.18 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0642
• Residual factor for significantly intense reflections: 0.051
• Weighted residual factors for significantly intense reflections: 0.1634
• Weighted residual factors for all reflections included in the refinement: 0.1695
• Goodness-of-fit parameter for all reflections included in the refinement: 1.095
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No