Information card for entry 4068796

Structure parameters

• Formula: C27 H47 Cu Li N O3
• Calculated formula: C27 H47 Cu Li N O3
• Title of publication: Gilman-Type versus Lipshutz-Type Reagents: Competition in Lithiocuprate Chemistry
• Authors of publication: Haywood, Joanna; Morey, James V.; Wheatley, Andrew E. H.; Liu, Ching-Yuan; Yasuike, Shuji; Kurita, Jyoji; Uchiyama, Masanobu; Raithby, Paul R.
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 1
• Pages of publication: 38
• a: 10.556 ± 0.002 Å
• b: 11.664 ± 0.002 Å
• c: 11.939 ± 0.002 Å
• α: 77.32 ± 0.03°
• β: 72.54 ± 0.03°
• γ: 85.82 ± 0.03°
• Cell volume: 1368 ± 0.5 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0537
• Residual factor for significantly intense reflections: 0.0456
• Weighted residual factors for significantly intense reflections: 0.118
• Weighted residual factors for all reflections included in the refinement: 0.126
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No