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Information card for entry 4068895
Preview
Coordinates | 4068895.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C68 H58 B Cl6 F4 P2 Rh |
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Calculated formula | C68 H58 B Cl6 F4 P2 Rh |
Title of publication | Can a Butadiene-Based Architecture Compete with its Biaryl Counterpart in Asymmetric Catalysis? Enantiopure Me-CATPHOS, a Remarkably Efficient Ligand for Asymmetric Hydrogenation |
Authors of publication | Doherty, Simon; Smyth, Catherine H.; Harriman, Anthony; Harrington, Ross W.; Clegg, William |
Journal of publication | Organometallics |
Year of publication | 2009 |
Journal volume | 28 |
Journal issue | 3 |
Pages of publication | 888 |
a | 11.6252 ± 0.0003 Å |
b | 22.6983 ± 0.0004 Å |
c | 11.7098 ± 0.0003 Å |
α | 90° |
β | 104.729 ± 0.002° |
γ | 90° |
Cell volume | 2988.36 ± 0.12 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 7 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.0507 |
Residual factor for significantly intense reflections | 0.0387 |
Weighted residual factors for significantly intense reflections | 0.0904 |
Weighted residual factors for all reflections included in the refinement | 0.0936 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.031 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4068895.html
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